EFFECT OF ACID ETCHING DURATIONS ON SHEAR BOND STRENGTH OF ADVANCED LITHIUM DISILICATE CERAMICS (An in-vitro study)

Document Type : Original Article

Authors

1 mti university

2 Fixed prosthodontics department, Faculty of Dentistry, Cairo University, Egypt

3 Cairo university

10.21608/acdj.2025.396282.1038

Abstract

Abstract
Introduction:The success of ceramic restorations relies heavily on the bond strength between ceramic and resin composites. Hydrofluoric acid(HF)etching is a critical step in surface treatment, yet its optimal duration for advanced lithium disilicate ceramics like CEREC Tessera remains unclear.
Objectives:This is vitro study aimed to assess how different HF etching times (20, 30, and 60 s) affect the shear bond strength between CEREC Tessera and resin composite substrates. it aims to evaluate the influence of etching time on failure modes.
Methodology: Twenty-four ceramic blocks (1.5 × 11 × 14 mm) were fabricated using CAD/CAM technology and randomly divided into three groups (n=8) based on HF etching duration: Group A (30 s), Group B (20 s), and Group C (60 s). All specimens were subjected to 5% HF etching, silane application,and bonding with dual-cure resin cement under a standardized load. After thermocycling (5,000 cycles),shear bond strength was tested using a universal testing machine. Failure modes were analyzed microscopically.Statistical analysis included one-way ANOVA, Chi-square tests,and normality assessments.
Results:Mean shear bond strengths were4.84 MPa(Group A), 4.91MPa (Group B),and5.32 MPa (Group C).No significant differences were found among groups p=0.90. Failure mode analysis revealed predominantly cohesive failures(>80%), with no statistically significant variation across groups p=0.39.
Conclusions:Within the limitations of this in vitro study, HF etching times ranging from 20 to 60 s did not significantly alter shear bond strength or failure patterns. The high incidence of cohesive failures indicates strong internal ceramic integrity and effective bonding
Keywords:CAD/CAM ceramics,CEREC Tessera,hydrofluoric acid etching,lithium disilicate,shear bond strength,thermocycling

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